KF-Al2O3催化合成2-甲基-1-苄基苯并咪唑

苯并咪唑类杂环化合物具有杀菌、消炎、抗癌、抗氧化的活性,广泛用于食品的防虫和防腐,用于动、植物病毒的防治,人体疾病和肿瘤的防治[1-3],本文用KF Al2O3作催化剂,用DMF为溶剂,利用2 甲基苯并咪唑与苄基溴反应合成2 甲基 1 苄基苯并咪唑的新型方法,考察了诸因素对产率的影响,找出了最佳的反应条件。合成路线如下:1　实验部分1 1　仪器与试剂Brurer AM 500超导核磁共振波谱仪(溶剂CDCl3);CarloErbal1106型元素分析仪,NicoletIm pact410型红外光谱仪,KBr压片,HP1100型和Finnigan FTMS 2000型质谱仪(以上均由华东理工大学分析…     

Robust Output Tracking Control of an Uncertain Linear System via a Modified Optimal Linear-Quadratic Method

This study investigates the robust output tracking problem for a class of uncertain linear systems. The uncertainties are assumed to be time invariant and to satisfy the matching conditions. According to the selected nominal parameters, an optimal solution with a prescribed degree of stability is determined. Then, an auxiliary input via the use of an adapting factor, connected to the nominal optimal control, is introduced to guarantee the robustness and prescribed degree of stability for the output tracking control of the uncertain linear systems. This method is very simple and effective and can reject bounded uncertainties imposed on the states. A maglev vehicle model example is given to show its effectiveness.     

Novel optical film sensor design based on p-polarized reflectance

A new scheme of optical film sensor is presented. The sensor is based on p-polarized reflectance, consisting of a sensing coated substrate, is easily optimized for maximum sensitivity in different applications. The resolutions of refractive index n_f, extinction coefficient k_f and thickness h_f of the sensitive films are predicted to be 10⁻⁷, 10⁻⁵ and 10⁻³ nm, respectively. Experimentally, we selected the sol–gel derived SnO₂ films as gas-sensitive films and conducted preliminary gas-sensing test. The results indicate that novel optical film sensor scheme has higher sensitivity, and the detection sensitivity is available to 10⁻¹ ppm on the condition of optimum optical parameters and incident angle.     

Synthesis of acetone oxime through acetone ammoximation over TS-1

The ammoximation of acetone to acetone oxime with 30 wt.% hydrogen peroxide over TS-1 has been studied. The conversion of acetone and the selectivity to acetone oxime can reach 99% and 94%, respectively. The by-products are the corresponding hydrazone, imine and small amounts of unidentified compounds. The influence of various parameters such as solvent, temperature, amounts of catalyst and the NH₃ to acetone molar ratio were investigated. This revised version was published online in August 2006 with corrections to the Cover Date.     

注入控制铜蒸气激光方向性时间过程测量

实验研究了注入控制对铜蒸气激光非稳腔输出光束质量的影响，从输出光发散角时间分辨过程的测量结果说明注入加速被注入腔内激光发散角的减小过程。由于被注入腔内放大自发辐射的存在，为得到较好的注入控制效果，注入光的脉宽和进入被注入腔的延时必须恰当。     

非本征型法布里-珀罗干涉仪光纤布拉格光栅应变温度传感器及其应用

介绍了光纤布拉格光栅非本征型法布里珀罗干涉仪集成复用传感器的结构、应变和温度同时监测的原理 ;观察到光纤布拉格光栅反射谱和非本征型法布里珀罗干涉仪干涉谱间的串扰 ,用 3dB带宽平均波长法减小了该串扰 ,提高了测量精度 ;将该传感器应用于三维编织复合材料的应变及温度同时监测。实验结果表明温度精度为± 1℃ ,应变精度为± 2 0 μ ,可满足实际应用的要求     

THE GLOBAL THEOREM OF A.N.BERLINSKII

ＳｏｃａｌｔｈｅＢｅｒｌｉｎｓｋｉｔｈｅｏｒｅｍｆｏｒｐｌａｎａｒｑｕａｄｒａｔｉｃＳｙｓｔｅｍ（ＱＳ）ｉｓ：ＴｈｅｏｒｅｍＡ［１］ＳｕｐｐｏｓｅｔｈａｔａＱＳｈａｓ４ｆｉｎｉｔｅｃｒｉｔｉｃａｌｐｏｉｎｔｓ（ＣＰｓ），Ｉｆｔｈｅｑｕａｄｒｉｌａ...     

Full field algebras, operads and tensor categories

We study the operadic and categorical formulations of (conformal) full field algebras. In particular, we show that a grading-restricted R×R-graded full field algebra is equivalent to an algebra over a partial operad constructed from spheres with punctures and local coordinates. This result is generalized to conformal full field algebras over VL⊗VR, where VL and VR are two vertex operator algebras satisfying certain finiteness and reductivity conditions. We also study the geometry interpretation of conformal full field algebras over VL⊗VR equipped with a nondegenerate invariant bilinear form. By assuming slightly stronger conditions on VL and VR, we show that a conformal full field algebra over VL⊗VR equipped with a nondegenerate invariant bilinear form exactly corresponds to a commutative Frobenius algebra with a trivial twist in the category of VL⊗VR-modules. The so-called diagonal constructions [Y.-Z. Huang, L. Kong, Full field algebras, arXiv: math.QA/0511328] of conformal full field algebras are given in tensor-categorical language.     

2006～201O年宁波非公有制经济领域人才需求预测

通过建立GM(1,1)模型,结合宁波市2005年对非公有制经济领域人才资源的抽样调查数据,对2006～2010年期间宁波市非公有制经济领域人才需求量和人才质量进行动态分析和预测.